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Extra info for Contrast Agents III: Radiopharmaceuticals – From Diagnostics to Therapeutics
Analogous oxo-alkoxide derivatives with rhenium (22) were prepared via ligand-exchange reactions, starting from [ReOCl4]– in basic media . In acidic media, the same reaction yields [ReOCl3(PNH2)] (23) . Interesting imido complexes, [MCl2(PN)(PNH)] [M is Re (24), Tc (25)], were obtained by reacting [NBu4][MOCl4] (M is Tc, Re) with an excess of PNH2 in nonpolar solvents . In all these six-coordinate complexes the PNH2 ligand always acts as bidentate, although it coordinates as neutral, monoanionic or dianionic, depending on the reaction conditions [36–38].
Salmain M, Gorfti A, Jaouen G (1998) Eur J Biochem 258:192 83. Wenzel M (1992) J Labelled Compd Radiopharm 31:641 84. Cesati RR, Tamagnan G, Baldwin RM, Zoghbi SS, Innis RB, Katzenellenbogen JA (1999) J Labelled Compd Radiopharm 42:S150 85. Spradau TW, Edwards WB, Anderson CJ, Welch MJ, Katzenellenbogen JA (1999) Nucl Med Biol 26:1 New Organometallic Technetium Complexes for Radiopharmaceutical Imaging 86. 87. 88. 89. 90. 91. 92. 93. 94. 95. 96. 97. 98. 99. 100. 101. 102. 103. 104. 105. 106. 107.
The results achieved in this field will be presented taking into account the 50 I. Santos et al. oxidation state of the metal (intermediate or low) and in each case the denticity and the donor atom set of the phosphines. 1 Mixed P, O Ligands The potentially bidentate (o-hydroxyphenyl)diphenylphosphine ligand (P1OH) reacts with [MOCl4]– yielding the mono oxocomplex [ReOCl3(P1O)]– (1) and the bisubstituted [MOCl(P1O)2] [M is Tc (2), Re (3)] (Scheme 1) [22, 23]. Complex 2 could also be obtained by a reduction/substitution reaction of pertechnetate with P1OH in the presence of HCl, while complex 3 was also synthesized by reacting the anionic trans-dioxo [ReO2(P1O)2]– with hydrochloric acid (Scheme 1) [23, 24].